Thermomechanical analysis (TMA) is used to study the properties of materials as a function of temperature.

MCL has a Netzsch 402 F1/F3 Hyperion TMA. The specs for the instrument are:

Maximum Force 3 N
Force Resolution < 0.1 mN
Displacement Resolution 0.125 nm
Temperature Range Steel furnace: -150 to 1,000 °C
Heating/cooling Rate 0.001 K/min. to 50 K/min.
Atmospheres Inert (Ar, N), oxidizing, reducing, vacuum

Sample size requirements

MCL is limiting TMA measurements to thermal expansion and shrinkage up to 1000C.  Size requirements are shown below. 

Temperature range Clamp (experiment) Type Maximum Dimensions
-150 to 1,000°C Expansion/penetration 12 mm (dia.); 30 mm (length)
TMA 402 F1 Hyperion
TMA 402 F1 Hyperion