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scintag x2 theta-theta powder diffractometer
SCINTAG 3 outside
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and inside views
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- Source: Copper, normal focus, glass
- Goniometer: Theta-theta; horizontal sample mount
- Angular range: 2-160 deg 2-theta
- Applications and Accessories:
- Bragg-Brentano parafocusing applications (loose powders, bulk solids, free-standing films, films on substrates)
- Grazing Incidence applications (thin films)
- High Temperature Stage (25 to1100 deg. C)
- Low Temperature Stage (25 to -196 deg. C)
- Sample Spinning (to improve particle statistics)
- Analyses:
- Phase Identification (Qualitative)
- Quantitative Analysis (RIR and Rietveld)
- Crystallinity Estimate
- Crystallite Size / Strain Estimate (Scherrer and Williamson-Hall techniques)
- Texture / Preferred Orientation (Rocking Curve)
- Lattice Parameter Determination
- Indexing
- Sample Preparation
- Powders
- A few grams of powder is always desirable, but often good patterns can be collected with milligram quantities
- Qualitative Analysis – 40 micron ideal (-325 mesh)
- Quantitative Analysis – 10 micron or less
- Bulk Solids, Pellets, Free-Standing films, Films on Substrates
- Maximum 1.1 inch width
- Maximum 3 inches length
- Maximum 0.5 inch thick